Microwave-assisted expeditious hydrolysis of isobenzofuranone derivatives using silica supported acid under organic solvent-free conditions

Loại tài liệu:

Article

Tác giả:

Safari, J.

Đề mục:

Arabian Journal of Chemistry

Nhà xuất bản:

Elsevier Ltd.

Ngày xuất bản:

October 2010

Định dạng:

pdf

Nguồn gốc:

Arabian Journal of Chemistry, Volume 4, Issue 1, January 2011, Pages 11-15

Ngôn ngữ:

eng

Lượt xem:

Lượt tải:

Nội dung

Silica sulfuric acid was found to be an efficient, reusable and environment-friendly catalyst for fast hydrolysis of various isobenzofuranone to corresponding 2-ketomethylquinoline derivatives in a high yield under solvent-free using microwave irradiation. As the activator of silica sulfuric acid the wet SiO2 was chosen. The reactions in conventional conditions were compared with the microwave assisted reactions. This approach can prove beneficial since the recovery of solvents from conventional reaction systems always results in some losses.

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Microwave-assisted expeditious hydrolysis of isobenzofuranone derivatives using silica supported acid under organic solvent-free conditions

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